Study Of The Effect Of Chemical Reduction Agent On The Synthesis And Structural Properties Of WO3-TeO2 And MoO3-TeO2 Two-dimensional Compounds. - Info and Reading Options
By Iranian journal of crystallography and mineralogy
"Study Of The Effect Of Chemical Reduction Agent On The Synthesis And Structural Properties Of WO3-TeO2 And MoO3-TeO2 Two-dimensional Compounds." and the language of the book is per.
“Study Of The Effect Of Chemical Reduction Agent On The Synthesis And Structural Properties Of WO3-TeO2 And MoO3-TeO2 Two-dimensional Compounds.” Metadata:
- Title: ➤ Study Of The Effect Of Chemical Reduction Agent On The Synthesis And Structural Properties Of WO3-TeO2 And MoO3-TeO2 Two-dimensional Compounds.
- Author: ➤ Iranian journal of crystallography and mineralogy
- Language: per
“Study Of The Effect Of Chemical Reduction Agent On The Synthesis And Structural Properties Of WO3-TeO2 And MoO3-TeO2 Two-dimensional Compounds.” Subjects and Themes:
- Subjects: ➤ Chemical reduction reaction - structural properties of WO3 - TeO2 - structural properties of MoO3 - TeO2 - optical properties - energy gap.
Edition Identifiers:
- Internet Archive ID: ijcmir-v-30n-1p-14-en-1
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"Study Of The Effect Of Chemical Reduction Agent On The Synthesis And Structural Properties Of WO3-TeO2 And MoO3-TeO2 Two-dimensional Compounds." Description:
The Internet Archive:
<span style="margin:0px;padding:0px;border:0px;font-size:14.6667px;line-height:inherit;font-family:'Times New Roman', serif;vertical-align:baseline;text-align:justify;background-color:rgb(255,255,255);">Preparation of two-dimensional nanostructures of WTe<sub style="margin:0px;padding:0px;border:0px;">2</sub> and MoTe<sub style="margin:0px;padding:0px;border:0px;">2</sub> by chemical solution synthesis methods is of great importance. In different synthesis methods, different precursors and concentrations are used. In this paper, we used the chemical reduction reaction method from solution for our analysis. Binary compounds of WO<sub style="margin:0px;padding:0px;border:0px;">3</sub> - TeO<sub style="margin:0px;padding:0px;border:0px;">2</sub> and MoO<sub style="margin:0px;padding:0px;border:0px;">3</sub> - TeO<sub style="margin:0px;padding:0px;border:0px;">2</sub> were prepared in two processes with reduction agents: (a) sodium borohydrate (NaBH<sub style="margin:0px;padding:0px;border:0px;">4</sub>) and (b) hydrazine in the presence of nitrogen gas. The structural and optical properties of the nanopowders were studied after chemical reduction. The results of X-ray diffraction (XRD) showed that in the WO<sub style="margin:0px;padding:0px;border:0px;">3</sub> - TeO<sub style="margin:0px;padding:0px;border:0px;">2</sub> binary compound, after chemical reduction with NaBH<sub style="margin:0px;padding:0px;border:0px;">4</sub>, the diffraction peaks of the TeO<sub style="margin:0px;padding:0px;border:0px;">2</sub> and WO<sub style="margin:0px;padding:0px;border:0px;">3</sub> binary compounds formed independently and after annealing in the presence of hydrazine, and the intensity of the peaks has been significantly increased. Field Emission Scanning Electron Microscopy (FE-SEM) images showed that the morphology of the nanoparticles was uniform in the form of spherical nanoparticles. In the combination of MoO<sub style="margin:0px;padding:0px;border:0px;">3</sub> - TeO<sub style="margin:0px;padding:0px;border:0px;">2</sub> with chemical reduction, other phases of Te<sub style="margin:0px;padding:0px;border:0px;">2</sub>O<sub style="margin:0px;padding:0px;border:0px;">5</sub> and TeMo<sub style="margin:0px;padding:0px;border:0px;">5</sub>O<sub style="margin:0px;padding:0px;border:0px;">16</sub> are formed in the shape of hemispheres, rods and polyhedrals, which indicates the formation of composite phases. The chemical bond structure and energy gap of samples were studied by FT-IR and UV-Vis spectroscopy</span><span dir="rtl" lang="fa" style="margin:0px;padding:0px;border:0px;font-weight:700;font-size:10pt;line-height:inherit;font-family:'Times New Roman', serif;vertical-align:baseline;text-align:justify;background-color:rgb(255,255,255);" xml:lang="fa"><span style="margin:0px;padding:0px;border:0px;font-style:inherit;font-variant:inherit;font-weight:inherit;font-size:inherit;line-height:inherit;font-family:'B Nazanin';vertical-align:baseline;"><span style="margin:0px;padding:0px;border:0px;font-style:inherit;font-variant:inherit;font-weight:normal;font-size:inherit;line-height:inherit;font-family:inherit;vertical-align:baseline;">.</span></span></span>
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