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"Niobium(V) Oxynitride: Synthesis, Characterization, And Feasibility As Anode Material For Rechargeable Lithium-Ion Batteries." and the language of the book is English.


“Niobium(V) Oxynitride: Synthesis, Characterization, And Feasibility As Anode Material For Rechargeable Lithium-Ion Batteries.” Metadata:

  • Title: ➤  Niobium(V) Oxynitride: Synthesis, Characterization, And Feasibility As Anode Material For Rechargeable Lithium-Ion Batteries.
  • Authors: ➤  
  • Language: English

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  • Internet Archive ID: pubmed-PMC3528069

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"Niobium(V) Oxynitride: Synthesis, Characterization, And Feasibility As Anode Material For Rechargeable Lithium-Ion Batteries." Description:

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This article is from <a href="//archive.org/search.php?query=journaltitle%3A%28Chemistry%20(Weinheim%20an%20Der%20Bergstrasse,%20Germany)%29" rel="nofollow">Chemistry (Weinheim an Der Bergstrasse, Germany)</a>, <a href="//archive.org/search.php?query=journaltitle%3A%28Chemistry%20(Weinheim%20an%20Der%20Bergstrasse,%20Germany)%29%20AND%20volume%3A%2818%29" rel="nofollow">volume 18</a>.<h2>Abstract</h2>Abstract: The decomposition reaction of niobium(V) oxytrichloride ammoniate to the oxynitride of niobium in the 5+ oxidation state was developed in a methodological way. By combining elemental analysis, Rietveld refinements of X-ray and neutron diffraction data, SEM and TEM, the sample compound was identified as approximately 5 nm-diameter particles of NbO1.3(1)N0.7(1) crystallizing with baddeleyite-type structure. The thermal stability of this compound was studied in detail by thermogravimetric/differential thermal analysis and temperature-dependent X-ray diffraction. Moreover, the electrochemical uptake and release by the galvanostatic cycling method of pure and carbon-coated NbO1.3(1)N0.7(1) versus lithium was investigated as an example of an Li-free transition-metal oxynitride. The results showed that reversible capacities as high as 250 and 80 A h kg−1 can be reached in voltage ranges of 0.05–3 and 1–3 V, respectively. Furthermore, a plausible mechanism for the charge–discharge reaction is proposed.

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